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44-46 In the presence of surface hydroxyl groups, that is, over a prereduced catalyst, CO 2 is converted to surface carbonate, which is first reduced to yield adsorbed CO and water Methanol is then generated via surface-bound formaldehyde and methoxy species, which is released from the surface as a result of hydrogenolysis or protolysis In contrast to the suggestion of Bell, surface formate is believed to be an intermediate for methane formation not involved in the reduction of CO 2 The activity of traditional ZnO-based catalysts may be improved by using new preparation methods Cu-ZnO-AI 20 3 catalysts prepared by a new oxalate gel precipitation exhibited higher activity in CO 2 reduction than did those made by coprecipitation, which was attributed to the isomorphous substitution of Cu and Zn.

47 ,48 New catalysts such as a Raney Cu-based system containing Zr49 and ultrafine CuB with Cr, Zr, and Th50 exhibit good characteristics The improved catalyst performance observed for a Cu-ZnO catalyst with added Pd is explained by the relative ease of hydrogen dissociation by the incorporated Pd particles and then spillover to the Cu-ZnO51 Catalysts with metals other than Cu have also been prepared and studied Ru on zeolite NaY prepared by ion-exchange and promoted with Co showed high activity for methanol production 52 Co showed a similar promoting effect when it was added to Rh on Si0253 The beneficial effect of Co was attributed to the stabilization of the CO species derived from the dissociation of CO 254 An iron-based FischerTropsch catalyst was mixed with a Cu-based catalyst and further doped with Pd and Ga to give a novel composite catalyst.

55 By selecting appropriate combinations of the components and reaction conditions, significant deviation from the SchulzFlory distribution could be achieved, which allowed the highly selective synthesis of ethanol New catalysts have been developed to afford coproduction of methanol and dimethyl ether, which requires the use of an active methanol synthesis catalyst and a solid acid component The transformation of methanol to dimethyl ether shifts the methanol formation equilibrium and thereby allows higher per-pass yields Hybrid catalysts composed of Cu-ZnO-Al203 and silica-alumina56 or Cu-ZnO-AI20rCr203 and H-ZSM-5 zeolite57 are active and stable catalysts Cu-Mo on H-ZSM-5 prepared by impregnation is also very effective in the production of dimethyl ether 58 Yields are usually low but high dimethyl ether selectivities are achieved..

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modes are shown in Figure 12-5 Typical breakage patterns showing the breakage of the main drop into orderly size daughter drops and the shedding of smaller drops from the tip ends of the main drop are given in Figure 12-6 Bentley and Leal (1986) and Stone et al (1986) studied deformation and breakup of a drop in a four-roll mill that allowed speci cation of idealized ows with various degrees of shear and extension In addition to determining the critical deformation rate under steady conditions, the following experiments were performed Drops were deformed to a steady nonspherical shape After stopping the ow motion, the stability of the drop was monitored as it relaxed to a sphere This enabled the conditions leading to breakup to be determined Tjahjadi and Ottino (1991) studied the breakup of drops subjected to both stretching and folding.

Setting Field Definitions All about field types Defining Calculation, Summary, and Global fields Understanding summary functions Setting Field Options Auto-enter options Data validation options Repeating fields Value lists Indexing and storage options Modifying Field Definitions, Names, and Options Changing field names Deleting a field and its data Duplicating fields Setting options for existing fields Changing a field s type Changing or deleting options for a field Summary 121 124 134 138 143 145 154 157 159 164 167 167 168 170 170 171 172 173.